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1-32 Part III
Part III Model 6600
Teledyne Analytical Instruments
Span Filter
This instrument employs a synthetic optical filter that can be operated
manually or automatically which simulates the absorption characteristics of the
required span fluid.
After the analyzer has been zeroed and spanned with known compositions
of the appropriate calibration fluids, the span filter is setup for manual or auto-
matic operation when introduced with a zero prepared fluid in the cell (Note: this
fluid may be clean air or N2 for very clean water stream applications, i.e., clean
condensates) and the appropriate equivalent absorption recorded. Use this
setting for all subsequent auto calibrations involving the span filter.
Sample System
Please refer to all pertinent sections of the 6600 Oil in Water manual for
operation of the Oil in water analyzer and sample system.
The sample system and analysis system are described in this manual.
5.6.4 Calibration by Correlation with Laboratory
Analysis
Because of the nature of the analysis, and the unique manner in which it
is accomplished, laboratory confirmation is recommended, particularly where
initial calibration was accomplished with oil not actually recovered from the
sample water.
The laboratory analytical method employed must be capable of detect-
ing both dissolved and undissolved oil fractions in the sample. We recom-
mend EPA method 413.1 (Replaced by method 1664A, gravemetric using
hexane extracting solvent) for sampling and analyzing as mentioned in
section 1.0 of the introduction.
Meaningful determination of the system’s capabilities requires precise
acquisition and processing of grab samples. Adhere to the following proce-
dures:
1. Insure that the system is functioning correctly as described
earlier in this manual.
2. Do not attempt to grab samples when the analyzer is indicating
drastic changes in oil concentration.
3. Draw two 1-gallon samples from the port for grab sample
opening V4 valve. Use clean containers, and fill alternately, not
- Model 6600 1
- Model 6600 2
- Oil in Water Analyzer 3
- Part I: iii 7
- Introduction 9
- 1.4 Operator Interface 10
- Part I: 1-5 13
- Installation 15
- 2-2: Part I 16
- Part I: 2-3 17
- 2-4: Part I 18
- Part I: 2-5 19
- 2-6: Part I 20
- Part I: 2-7 21
- Table 2-3: RS-232 Signals 21
- 2-8: Part I 22
- Part I: 2-9 23
- 2.3 Testing the System 23
- 2-10: Part I 24
- Operation 25
- 3-2 Part I 26
- Part I 3-3 27
- 3-4 Part I 28
- 3.3 The System Function 28
- Part I 3-5 29
- 3-6 Part I 30
- Part I 3-7 31
- 3-8 Part I 32
- Part I 3-9 33
- 3-10 Part I 34
- Part I 3-11 35
- 3-12 Part I 36
- Part I 3-13 37
- 3-14 Part I 38
- Part I 3-15 39
- 3-16 Part I 40
- Part I 3-17 41
- 3-18 Part I 42
- Part I 3-19 43
- 3-20 Part I 44
- Part I 3-21 45
- 3-22 Part I 46
- 3.5 The Alarms Function 46
- Part I 3-23 47
- 3-24 Part I 48
- Part I 3-25 49
- 3-26 Part I 50
- Part I 3-27 51
- 3.7 The Analyze Function 51
- 3-28 Part I 52
- 3.8 Programming 52
- Part I 3-29 53
- 3-30 Part I 54
- Part I 3-31 55
- UP/DOWN key to 55
- 3-32 Part I 56
- Maintenance 57
- 4-2: Part I 58
- Part I: 4-3 59
- 4.3 Major Internal Components 59
- 4-4: Part I 60
- Part II: iii 63
- Operational Theory 65
- 1-2 Part II 66
- 1.2 Optical Bench 66
- Part II: 1-3 67
- 1.3 Photometer Amplifier 67
- 1-4 Part II 68
- 1.4 Automatic Zero System 68
- Part II: 1-5 69
- 1.5 System Description 69
- 1-6 Part II 70
- 1.6 Photometer 70
- Part II: 1-7 71
- 1-8 Part II 72
- 1.7 Sample Systems 72
- 2-2: Part II 74
- Part II: 2-3 75
- 2.4 Calibration 75
- 2.4.1 Calibration Fluids 75
- 2-4: Part II 76
- 3-2 Part II 78
- Part II 3-3 79
- 3-4 Part II 80
- Part II 3-5 81
- 3-6 Part II 82
- Part II 3-7 83
- 3-8 Part II 84
- Part II 3-9 85
- 3-10 Part II 86
- Part III: iii 89
- Part III: 1-1 91
- 1.0 Introduction 91
- 1-2 Part III 92
- 2.0 The Method of Analysis 92
- 2.1 The Optical Bench 92
- 2.2 The Photometer Amplifier 92
- Part III: 1-3 93
- 1-4 Part III 94
- 2.3 The Automatic Zero System 94
- Part III: 1-5 95
- 1-6 Part III 96
- Part III: 1-7 97
- 1-8 Part III 98
- 3.0 System Description 98
- Part III: 1-9 99
- 3.1 Photometer 99
- 3.1.1 Source Module 99
- 3.1.2 Sample Cell 99
- 1-10 Part III 100
- Model 6600 100
- 3.1.3 Detector Module 100
- 3.1.4 Control/Analysis Unit 100
- Part III: 1-11 101
- 3.3 Electrical Connections 101
- 3.4 The Sampling System 101
- 1-12 Part III 102
- Part III: 1-13 103
- Homogenizing 103
- 1-14 Part III 104
- Part III: 1-15 105
- 1-16 Part III 106
- 3.5 The Signal Outputs 106
- 3.6 Recorder Requirement 106
- Part III: 1-17 107
- 3.7 The Process Alarm System 107
- 3.8 The amplifier PCB 107
- 3.8.1 Auto Zero Circuit 107
- 1-18 Part III 108
- 3.8.2 Signal Failure Alarm 108
- Part III: 1-19 109
- 4.0 INSTALLATION 109
- Part III: 1-21 111
- 4.1.5 Sample Delivery System 111
- 4.1.6 Safe Vent (Drainage) 111
- 1-22 Part III 112
- 5.1 Installation Check 112
- 5.2 Electronics Check 112
- Part III: 1-23 113
- 5.3 Electrical Check 113
- 5.4 Sample Delivery Check 113
- 1-24 Part III 114
- Part III: 1-25 115
- 1-26 Part III 116
- Part III: 1-27 117
- 1-28 Part III 118
- Part III: 1-29 119
- 5.6.1 Zero Fluid Preparation 119
- 5.6.2 Span Fluid Preparation 119
- 1-30 Part III 120
- 5.6.3 Calibration 120
- Part III: 1-31 121
- 1-32 Part III 122
- Analysis 122
- Part III: 1-33 123
- homogenizer 124
- Part III: 1-35 125
- CORRELATION 125
- 1-36 Part III 126
- OPERATIONAL DUTIES 126
- Part III: 1-37 127
- 6.2 Routine Maintenance 127
- 1-38 Part III 128
- (Application dependent) 128
- Part III: 1-39 129
- 7.0 SERVICE PROCEDURES AND 129
- ADJUSTMENTS 129
- End Amplifiers 129
- 1-40 Part III 130
- Part III: 1-41 131
- 7.4 The Inverting Amplifier 131
- 1-42 Part III 132
- 7.6 Sample Cell Maintenance 132
- Part III: 1-43 133
- 7.7 Sample System Maintenance 133
- 7.8 Zero Filter Replacement 133
- 1-44 Part III 134
- Part III: 1-45 135
- 7.10 Lamp Replacement 135
- 7.11 Phototube Replacement 135
- Part III: 1-47 137
- 8.2.2 Sample Pump Failure 137
- 8.3 Zero Drift Problems 137
- 1-48 Part III 138
- Part III: 1-49 139
- 1-50 Part III 140
- Oil in Water Part III 141
- 1-52 Part III 142
- (see addendum 142
- (see addendum drawings) 142
- Part III: 1-53 143
- 1-54 Part III 144
- Part III: 1-55 145
- 1-56 Part III 146
- Part III: 1-57 147
- Appendix 148
- (non freezing, non-boiling) 149
- Model 6600 150
- Generic Drawing List 151
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