Teledyne 6700-C Total Organic Carbon Analyzer (Hi-Temp Comb User Manual

Teledyne Analytical Instruments OPERATING INSTRUCTIONS FOR Model 6700C High Temperature Combustion Online TOC Analyzer DANGER Depending upon you

Model 6700C TOC Teledyne Analytical Instruments x 4.4.2 Reagents 344.4.2.1 Preparation Of Sulfuric Acid Solution 344.4.3 NDIR Calibration (

High Temperature Combustion Teledyne Analytical Instruments xi List of Figures Figure 2-1 Typical Flow Diagram ...

Model 6700C TOC Teledyne Analytical Instruments xii List of Tables Table 3-1: Preparation of Standards (TOC) ...

High Temperature Combustion Teledyne Analytical Instruments xiii DANGER COMBUSTIBLE GAS USAGE WARNING This is a general purpose instrument

High Temperature Combustion Operational Theory Teledyne Analytical Instruments 15 Introduction 1.1 Overview Teledyne Analytical Instruments (TAI

Operational Theory Model 6700C TOC Teledyne Analytical Instruments 16 The Analyzer is designed for monitoring of Total Organic Carbon (TOC) in w

High Temperature Combustion Operational Theory Teledyne Analytical Instruments 17 Operational Theory 2.1 Measurement Principle Refer to Figure 2

Operational Theory Model 6700C TOC Teledyne Analytical Instruments 18 Figure 2-1 Typical Flow Diagram

High Temperature Combustion Installation/Startup Teledyne Analytical Instruments 19 Installation and Startup The Model 6700C is often configured

Model 6700C TOC Teledyne Analytical Instruments ii Copyright © 2012 Teledyne Instruments/ Analytical Instruments All Rights Reserved. No part of

Installation/Startup Model 6700C TOC Teledyne Analytical Instruments 20 Figure 3-1: Combustion Module Interior 3.2 Non – Catalytic Reactor Pa

High Temperature Combustion Installation/Startup Teledyne Analytical Instruments 21 Quartz Combustion Reactor (P/N: R3332) Ceramic Wool Disk

Installation/Startup Model 6700C TOC Teledyne Analytical Instruments 22 Glass Reactor Top (P/N: R3331) Top Retainer (P/N: R3350) 3.2.2 Prepa

High Temperature Combustion Installation/Startup Teledyne Analytical Instruments 23 3.2.2.1 INSTALL QUARTZ SLEEVE (INSERT) Carefully place the Q

Installation/Startup Model 6700C TOC Teledyne Analytical Instruments 24 CAUTION: Be careful to slowly place the assembly in a vertical position,

High Temperature Combustion Installation/Startup Teledyne Analytical Instruments 25 3.4 Inserting Reactor into Furnace Carefully insert

Installation/Startup Model 6700C TOC Teledyne Analytical Instruments 26 Figure 3-6: Filling Separator with DI Water  Prepare to position Glass

High Temperature Combustion Installation/Startup Teledyne Analytical Instruments 27 Figure 3-8: Top Retainer Installation 3.5 Startup of

Installation/Startup Model 6700C TOC Teledyne Analytical Instruments 28 CAUTION: FAILURE TO OBSERVE THIS WILL RESULT IN IMPROPER OPERATION OR A

High Temperature Combustion Operation Teledyne Analytical Instruments 29 Operation After proper installation the instrument must be calibrated.

High Temperature Combustion Teledyne Analytical Instruments iii Specific Model Information Instrument Serial Number: _______________________

Operation Model 6700C TOC Teledyne Analytical Instruments 30 Although your analyzer has been configured for optimum performance in your applica

High Temperature Combustion Operation Teledyne Analytical Instruments 31 4.3.1 Edit/Parameters From the EDIT Menu, select: [Parameters]. The f

Operation Model 6700C TOC Teledyne Analytical Instruments 32 4.3.2 Edit/Alarms The next recommended settings to be verified or set are the Alarm

High Temperature Combustion Operation Teledyne Analytical Instruments 33 Table 3-1: Preparation of Standards (TOC) ORGANIC COMPOUNDS 100 mg/Lite

Operation Model 6700C TOC Teledyne Analytical Instruments 34 4.4.2 Reagents The following provides reagent preparation guides for acid reagent. S

High Temperature Combustion Operation Teledyne Analytical Instruments 35 The following screen appears: Disconnect the tubing from the GLS an

Operation Model 6700C TOC Teledyne Analytical Instruments 36 To set IR “Zero”:  Flow 200cc/minute oxygen (or CO2 free air) for 5 minutes.  Al

High Temperature Combustion Operation Teledyne Analytical Instruments 37 Select [Liquid]. The following screen appears: Select “ZERO”. D. I

Operation Model 6700C TOC Teledyne Analytical Instruments 38 4.5.1 Scale Select [Scale] to edit the scale displayed. The following screen will

High Temperature Combustion Operation Teledyne Analytical Instruments 39 Using the Scroll Bar, select the data to be viewed. 4.5.3 Historical

Model 6700C TOC Teledyne Analytical Instruments iv Safety Messages Your safety and the safety of others is very important. We have provided many

Operation Model 6700C TOC Teledyne Analytical Instruments 40 Select [System Diagnostics]. The following menu appears: From this screen th

High Temperature Combustion Maintenance Teledyne Analytical Instruments 41 Maintenance Aside from normal cleaning and checking for leaks at the

Maintenance Model 6700C TOC Teledyne Analytical Instruments 42 Table 5-1 Troubleshooting PROBLEMS SOLUTION Analyzer will not turn on Check fuse

High Temperature Combustion Maintenance Teledyne Analytical Instruments 43 To remove and service the NDIR, follow the illustrated sequence as de

Maintenance Model 6700C TOC Teledyne Analytical Instruments 44  Remove insulation from IR Cell.  Remove lock-tight from three thumbnuts and

High Temperature Combustion Maintenance Teledyne Analytical Instruments 45  Remove IR Cell Assembly Note: a. ‘O’-Rings in each of Detecto

Maintenance Model 6700C TOC Teledyne Analytical Instruments 46  *Remove ‘O’-Ring and Sapphire window taking care to avoid scratching sapphire w

High Temperature Combustion Maintenance Teledyne Analytical Instruments 47 5.3.3 Master Interface Board (P/N B718 & P/N B717)

Maintenance Model 6700C TOC Teledyne Analytical Instruments 48 3. Disconnect connectors. 4. Slide Power Supply off the Din Rail. 5. Remove Pow

High Temperature Combustion Maintenance Teledyne Analytical Instruments 49 6. 6. Recalibrate liquid Zero and Span. Figure 5-4: Removing Co

High Temperature Combustion Teledyne Analytical Instruments v This manual provides information designed to guide you through the installation,

Maintenance Model 6700C TOC Teledyne Analytical Instruments 50 Figure 5-5: Reactor Assembly and GLS 3. Remove GLS.  Loosen fitting.  Raise

High Temperature Combustion Maintenance Teledyne Analytical Instruments 51 6. Tilt black plate forward. 7. Remove Reactor after complete cool-

Maintenance Model 6700C TOC Teledyne Analytical Instruments 52 Procedure: 1. Shut off Power to Instruments. 2. Shut off all gas to analyzer and

High Temperature Combustion Maintenance Teledyne Analytical Instruments 53 Procedure: 1. Turn carrier gas (Air/O2) OFF. 2. Turn Pumps OFF. 3.

Maintenance Model 6700C TOC Teledyne Analytical Instruments 54 Procedure: CAUTION: OBSERVE NORMAL PRECAUTIONS WHEN HANDLING ACIDS. Replaceme

High Temperature Combustion Maintenance Teledyne Analytical Instruments 55 Figure 5-9: Injector Assembly

Maintenance Model 6700C TOC Teledyne Analytical Instruments 56

Percent Oxygen Analyzer Appendix Teledyne Analytical Instruments 57 Appendix A.1 Specifications (The following specifications are nominal and

Appendix Model 3290 Teledyne Analytical Instruments 58 Drain: Gravity drain, vented to atmosphere. Suspended Solids: 400 microns (max.) Re

Percent Oxygen Analyzer Appendix Teledyne Analytical Instruments 59 Send orders to: TELEDYNE Analytical Instruments 16830 Chestnut Street City o

Model 6700C TOC Teledyne Analytical Instruments vi

High Temperature Combustion Teledyne Analytical Instruments vii Additional Safety Information All relevant precautions and safety remarks of th

Model 6700C TOC Teledyne Analytical Instruments viii Responsibilities & Duties of the End User The end user is responsible to ensure that on

High Temperature Combustion Teledyne Analytical Instruments ix Table of Contents Additional Safety Information .........